3,5-Difluoropyridine → HCID 11573675, compound

HRID 2219478Notes

Reaction equation

HRID 2219478 reaction equation
[F:1][C:2]1[CH:3]=[CH:4][C:5]([NH:8][C:9]([C:11]2[C:16]([NH2:17])=[CH:15][CH:14]=[C:13]([CH3:18])[N:12]=2)=[O:10])=[N:6][CH:7]=1.[F:19][C:20]1[CH:21]=[N:22][CH:23]=[C:24](F)[CH:25]=1>>[F:1][C:2]1[CH:3]=[CH:4][C:5]([NH:8][C:9]([C:11]2[C:16]([NH:17][C:24]3[CH:23]=[N:22][CH:21]=[C:20]([F:19])[CH:25]=3)=[CH:15][CH:14]=[C:13]([CH3:18])[N:12]=2)=[O:10])=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 6428203,5-DifluoropyridineHCID 86607569HCID 86607569, compound

Product 1

HCID 11573675HCID 11573675, compound

Procedure

The title compound, light yellow solid, MS (ISP): m/e=342.1 (M+H+), was prepared from 3-Amino-6-methyl-pyridine-2-carboxylic acid (5-fluoro-pyridin-2-yl)-amide and 3,5-Difluoropyridine in accordance with the general method of example 7.

Sources & evidence

ORD record
ord-934a7e887de1430496a0a278576b43ce
Source dataset
uspto-grants-2008_08
Patent number
US07414060B2

Reaction notes

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