HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3,5-difluorobenzene → HCID 86607578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3,5-difluorobenzene | HCID 136313 | — |
| Reactant | HCID 11522606 | HCID 11522606 | — |
| Product | HCID 86607578 | HCID 86607578 | — |
Reaction Steps
The title compound, was prepared from 3-Amino-6-methyl-pyridine-2-carboxylic acid (2-methyl-pyridin-4-yl)-amide (example 5) in accordance with the general method of example 20 using 1-Bromo-3,5-difluorobenzene instead of 3-Bromo-4-methylpyridine to yield the final compound as a yellow crystalline solid, MS (ISP): m/e=355.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414060B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-25dcb3fa6a2446b0aff1371940a06cc1 |
| Source note | uspto-grants-2008_08 |