HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-6-methylpyrazine → 6-Methyl-3-(6-methyl-pyrazin-2-ylamino)-pyridine-2-carboxylic acid (1-methyl-1H-pyrazol-3-yl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-6-methylpyrazine | HCID 12236939 | — |
| Reactant | 3-Bromo-6-methyl-pyridine-2-carboxylic acid (1-methyl-1H-pyrazol-3-yl)-amide | HCID 86607590 | — |
| Product | 6-Methyl-3-(6-methyl-pyrazin-2-ylamino)-pyridine-2-carboxylic acid (1-methyl-1H-pyrazol-3-yl)-amide | HCID 11529891 | — |
Reaction Steps
The title compound, was prepared from 3-Bromo-6-methyl-pyridine-2-carboxylic acid (1-methyl-1H-pyrazol-3-yl)-amide in accordance with the general method of Example 78, step 3 using 2-Amino-6-methylpyrazine instead of 3-Amino-1-methyl-pyrazole to yield the final compound as a brown solid, MS (ISP): m/e=324.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414060B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-ed6811f34a334acf8bf2f2e85cc41925 |
| Source note | uspto-grants-2008_08 |