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2-Methyl-1,3-thiazol-4-amine → 6-Methyl-3-(5-methyl-pyridin-3-ylamino)-pyridine-2-carboxylic acid (2-methyl-thiazol-4-yl)-amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methyl-1,3-thiazol-4-amine | HCID 14772700 | — |
| 反応物 | 6-Methyl-3-(5-methyl-pyridin-3-ylamino)-pyridine-2-carboxylic acid ethyl ester | HCID 69236773 | — |
| 生成物 | 6-Methyl-3-(5-methyl-pyridin-3-ylamino)-pyridine-2-carboxylic acid (2-methyl-thiazol-4-yl)-amide | HCID 11544635 | — |
反応手順
The title compound, was prepared from 6-Methyl-3-(5-methyl-pyridin-3-ylamino)-pyridine-2-carboxylic acid ethyl ester and 4-Amino-2-methylthiazole in accordance with the general method of Example 78, step 2 to yield the final compound as a light-yellow solid, MS (ISP): m/e=340.1 (M+H+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07414060B2 |
| 出典データセット | uspto-grants-2008_08 |
| ORD ID | ord-3364b361cba149b7940241c028849c5f |
| 出典メモ | uspto-grants-2008_08 |