HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4-Dimethylcyclohexen-1-ylboronic acid → 5-[4-Amino-3-(4,4-dimethyl-cyclohex-1-enyl)-phenyl]-1,3-dimethyl-tetrahydro-pyrimidin-2-ylidene-cyanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4-Dimethylcyclohexen-1-ylboronic acid | HCID 44119555 | — |
| Reactant | 5-(4-Amino-3-bromo-phenyl)-1,3-dimethyl-tetrahydro-pyrimidin-2-ylidene-cyanamide | HCID 86615904 | — |
| Product | 5-[4-Amino-3-(4,4-dimethyl-cyclohex-1-enyl)-phenyl]-1,3-dimethyl-tetrahydro-pyrimidin-2-ylidene-cyanamide | HCID 86615903 | — |
Reaction Steps
The title compound was prepared according to the Suzuki coupling procedure of Example 3, step (a), using 4,4-dimethyl-cyclohex-1-enyl boronic acid and 5-(4-amino-3-bromo-phenyl)-1,3-dimethyl-tetrahydro-pyrimidin-2-ylidene-cyanamide Mass spectrum (ESI, m/z): Calcd. for C21H29N5, 352.2 (M+H). found 352.4
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414050B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-9af7ded72f514768938ad597143a4e75 |
| Source note | uspto-grants-2008_08 |