HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 69224807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Chloro-3-(trifluoromethyl)pyridine | HCID 589833 | — |
| Reactant | N-(4-tert-butylphenyl)-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidin-4-amine | HCID 59021490 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69224807 | HCID 69224807 | — |
Reaction Steps
The title compound was prepared using the general procedure set forth in Example 3, above, by heating a mixture of 2-chloro-3-(trifluoromethyl)pyridine (0.108 g, 0.59 mmol), N-(4-tert-butylphenyl)-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidin-4-amine (Example 3.A) (0.112 g, 0.40 mmol) and potassium carbonate (0.16 g, 1.19 mmol) in DMF (2 mL) for 1 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414131B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-f31e7d26c116478897f58c8b98250a3b |
| Source note | uspto-grants-2008_08 |