Potassium Carbonate → HCID 17980976, compound

Participants

Reaction Steps

A mixture of 2.80 g (8.68 mmol) of the compound obtained in Step 1, 8.18 g (26.0 mmol) of 1,11-Dibromo-undecane, 3.66 g ((26.0 mmol) of K2CO3 and 40 mL of dry butanone is refluxed for 24 h, then the reaction mixture is allowed to return to room temperature. The mixture is filtered and the solvent is distilled off under reduced pressure. The resulting crude is purified by column chromatography on silica gel using CH2Cl2 as eluent to give a pure white solid (9.11 g, 41% yield).

Provenance & Evidence