Methanesulfonyl chloride → HCID 71653293, compound

HRID 2220088Notes

Reaction equation

HRID 2220088 reaction equation
[CH2:1]([N:4]1[CH2:9][CH2:8][N:7]([C:10]2[CH:11]=[C:12]([OH:16])[CH:13]=[CH:14][CH:15]=2)[CH2:6][CH2:5]1)[CH2:2][CH3:3].[CH3:17][S:18](Cl)(=[O:20])=[O:19].C([O-])(=O)/C=C/C([O-])=O>>[CH2:1]([N:4]1[CH2:9][CH2:8][N:7]([C:10]2[CH:11]=[C:12]([O:16][S:18]([CH3:17])(=[O:20])=[O:19])[CH:13]=[CH:14][CH:15]=2)[CH2:6][CH2:5]1)[CH2:2][CH3:3]

Participants

4

Reactant 3

HCID 31297Methanesulfonyl chlorideHCID 5460307FumarateHCID 22397846HCID 22397846, compound

Product 1

HCID 71653293HCID 71653293, compound

Procedure

Beginning with 3-(4-propyl-piperazin-1-yl)-phenol and methanesulfonyl chloride: m.p 143-144° C. (fumarate); MS m/z (rel. intensity, 70 eV) 298 (M+, 35), 269 (95), 121 (25), 84 (30), 70 (bp);

Sources & evidence

ORD record
ord-461229708c0747f585ab16a53cd7fe71
Source dataset
uspto-grants-2008_08
Patent number
US07417043B2

Reaction notes

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