HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2,4-Difluorophenyl)methanethiol → Ethyl 6-[(2,4-difluorobenzyl)sulfanyl]-1-cyclohexene-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2,4-Difluorophenyl)methanethiol | HCID 2761425 | — |
| Reactant | ethyl 6-[N-(2,4-difluorophenyl)sulfamoyl]-1-cyclohexene-1-carboxylate | HCID 9928140 | — |
| Product | Ethyl 6-[(2,4-difluorobenzyl)sulfanyl]-1-cyclohexene-1-carboxylate | HCID 22026122 | 45% |
Reaction Steps
In the same manner as in Reference Example 1, ethyl 6-[N-(2,4-difluorophenyl)sulfamoyl]-1-cyclohexene-1-carboxylate (455 mg) and (2,4-difluorophenyl)-methanethiol (421 mg) were reacted to give ethyl 6-[(2,4-difluorobenzyl)sulfanyl]-1-cyclohexene-1-carboxylate (185 mg) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417059B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-2582060741dc429fb5236c737ac4d01f |
| Source note | uspto-grants-2008_08 |