HCID 68895015, compound → HCID 59772414, compound

Participants

Reaction Steps

To a solution of Example 295 (50 mg, 0.16 mmol) in MeOH (10 mL) was added palladium hydroxide (25 mg). The solution was stirred under a hydrogen atmosphere for 3 hours. The mixture was filtered through a nylon membrane filter, concentrated and recrystallized from EtOAc/hexane to give the title compound as a white solid (35 mg, 69%). HPLC Rt=3.56 min. m/z=319(M+H+).

Provenance & Evidence