HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Benzyl-methyl-amino)-heptan-3-one → 1-[Benzyl(methyl)amino]-3-hexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Benzyl-methyl-amino)-heptan-3-one | HCID 17981922 | — |
| Reactant | HCID 178455855 | HCID 178455855 | — |
| Product | 1-[Benzyl(methyl)amino]-3-hexanone | HCID 419586 | — |
Reaction Steps
Using a method similar to that for 1-(Benzyl-methyl-amino)-heptan-3-one, propylmagnesium chloride (2 M solution in diethyl ether) affords the title compound: mass spectrum (ion spray) m/z=220 (M+1): 1H NMR (CDCl3) δ 7.35-7.24 (m, 5H), 3.51 (s, 2H), 2.74-2.69 (m, 2H), 2.66-2.61 (m, 2H), 2.39 (t, 2H), 2.20 (s, 3H), 1.67-1.57 (m, 2H), 0.92(t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417064B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-5981ee199ffe46258ddf07838c48ee81 |
| Source note | uspto-grants-2008_08 |