HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Benzyl-methyl-amino)-5-methyl-hexan-3-ol → 1-(Benzyl-methyl-amino)-4-methyl-pentan-3-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Benzyl-methyl-amino)-5-methyl-hexan-3-ol | HCID 17981919 | — |
| Reactant | HCID 178418918 | HCID 178418918 | — |
| Product | 1-(Benzyl-methyl-amino)-4-methyl-pentan-3-ol | HCID 17981939 | — |
Reaction Steps
Using a method similar to that for 1-(Benzyl-methyl-amino)-5-methyl-hexan-3-ol, isopropylmagnesium chloride affords the title compound: mass spectrum (ion spray) m/z=222.1(M+1); 1H NMR (CDCl3) δ 7.34-7.23 (m, 5H), 6.21 (br s, 1H), 3.63 (d, 1H), 3.51-3.47 (m, 1H), 3.42 (d, 1H), 2.81-2.74 (m, 1H), 2.59-2.54 (m, 1H), 2.19 (s, 3H), 1.72-1.47 (m, 3H), 0.95 (d, 3H), 0.89 (d, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417064B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-98a62b5a5aba4aa0bb520ae700fd876c |
| Source note | uspto-grants-2008_08 |