Carbon tetrabromide → HCID 58346788, compound

Participants

Reaction Steps

This compound was prepared in a similar fashion as described in Example 48 step 5 starting from 2-{6[2-(4-nitro-phenyl)-ethoxy]-4,5-dihydro-10-thia-2,3,7,9-tetraaza-cyclopenta[a]fluoren-3-yl}-ethanol (4.2 g, 9.6 mmol), carbontetrabromide (6.37 g, 19.20 mmol), and triphenyl phosphine (5.03 g, 19.20 mmol). The desire product was obtained as a light yellow solid (2.6 g) in 54% yield. LCMS RT=3.55 min; [M+H]+=500.1/502.0.

Provenance & Evidence