HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86611770, compound → [2-Isopropyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86611770 | HCID 86611770 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | [2-Isopropyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]acetic acid | HCID 23134282 | 83.8% |
Reaction Steps
To a solution of benzyl[2-isopropyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]acetate (0.238 g) in ethanol (10 mL) was added 10% palladium-carbon (0.05 g), and the mixture was stirred at room temperature for 2 hrs under an atmosphere of hydrogen. The catalyst was removed by filtration, and the solvent was evaporated under reduced pressure to afford the title compound (0.156 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417169B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-a22591657683410996d50e021f08c8f0 |
| Source note | uspto-grants-2008_08 |