HuagongsheHuagongshe Chemistry Print Report · For research reference only
beta-Bromostyrene → HCID 86600771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | beta-Bromostyrene | HCID 7667 | — |
| Reactant | 2,3,4,5-Tetraphenyl-2-cyclopenten-1-one | HCID 280487 | — |
| Reactant | HCID 178506700 | HCID 178506700 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86600771 | HCID 86600771 | — |
Reaction Steps
1,2,4,5-Tetraphenyl-3-p-vinylphenylcyclopenta-1,3-diene was prepared from 37.8 g (0.098 mol) of 2,3,4,5-tetraphenylcyclopent-2-enone and 0.5 mol of p-vinylphenyllithium (from 7 g (1 mol) of Li and 91.52 g (0.5 mol of bromostyrene) in 300 ml of ether and was purified analogously to 1,2,3,4-tetraphenyl-5-p-vinylphenylcyclopenta-1,3-diene. (Yield: 37 g (80%))
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417247B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-38e0867afb0f4819a1f7be70b4e3a667 |
| Source note | uspto-grants-2008_08 |