HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Quinolinecarboxaldehyde → HCID 59773021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Quinolinecarboxaldehyde | HCID 83641 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 51898061 | HCID 51898061 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59773021 | HCID 59773021 | 9.1% |
Reaction Steps
Experimental condition analogous to Example 1, from (S)—C-(1-cyclohexylmethyl-pyrrolidin-2-yl)-methylamine 0.25 g (1.3 mmol), quinoline-3-carbaldehyde 0.2 g (1.3 mmol), sodium triacethoxyborohydride 0.53 g (2.6 mmol), and molecular sieve in 8 mL dichloromethane. Yield to 40 mg of compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417062B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-19a22bc946c447e0b6339026639ec050 |
| Source note | uspto-grants-2008_08 |