反应详情

A mixture of 1.0 eq. of 19 and 0.1 wt/wt eq. of 10% Pd on carbon was hydrogenated at 10-60 psi of hydrogen for a time sufficient for reaction completion. The reaction mixture was filtered through Celite. The filtrate was concentrated by rotary evaporation. The crude material was dried under vacuum to give product 20.

1. filtrationThe reaction mixture was filtered through Celite
2. concentrationThe filtrate was concentrated by rotary evaporation
3. dry with materialThe crude material was dried under vacuum