HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 2,5,8,11,14,17,20,23,26,29-Decaoxahentriacontan-31-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Triethylene Glycol | HCID 8172 | — |
| Reactant | m-PEG7-Ms | HCID 21930814 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2,5,8,11,14,17,20,23,26,29-Decaoxahentriacontan-31-ol | HCID 14550547 | — |
Reaction Steps
Monodispersed compound 32 was prepared from compound 31 and monodispersed triethylene glycol using the procedure described above in Example 17. Oil; Rf 0.41 (methanol: chloroform=6:10); MS m/z calc'd for C21H44O11 472.29 (M++1), found 472.29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07368260B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-783ff6d15d5d4dcd91d81b830e764a32 |
| Source note | uspto-grants-2008_05 |