HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 21947121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Sulfate | HCID 24436 | — |
| Reactant | TRIPLAL | HCID 3034463 | — |
| Product | HCID 21947121 | HCID 21947121 | — |
Reaction Steps
To a 0° C. stirred solution of 66 g (0.47 mol) triplal and 21 g sodium sulfate in 150 mL of methanol is added 29 g (0.47 mol) of ethanolamine. The reaction is allowed to warm to room temperature. After stirring for 24 h the mixture is cooled to 0° C. and the solids are removed via vacuum filtration through Celite. Evaporation of the solvent gives a clear, slightly yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07368415B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-f2625d76c80d4caaadc3f547dd33b743 |
| Source note | uspto-grants-2008_05 |