HRID2221131

反应详情

EQUATION

反应方程式

HRID 2221131 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A suspension of 4-chlorophenol (2.6 g, 20 mmol), chloroacetone (2.8 g, 30 mmol) and potassium carbonate (3.45 g, 25 mmol) in acetone (100 ml) is heated at reflux for 3 hours. The precipitating inorganic salts are filtered off and the filtrate is evaporated to dryness to give the 1-(4-chlorophenoxy)-propan-2-one.

WORKUP

后处理

  1. temperatureis heated
  2. temperatureat reflux for 3 hours
  3. filtrationThe precipitating inorganic salts are filtered off
  4. customthe filtrate is evaporated to dryness