2,3,5-Triiodobenzoic acid → HCID 178436117, compound

Participants

Reaction Conditions

Reaction Steps

1980 g of toluene were used as initial charge in a 15 l stirred tank at 25° C., and y1 g of styrene and y2 g of the 12% strength by weight solution of s-BuLi in cyclohexane were added with stirring. 10 min after this, 913 g of the 20% strength by weight solution of TIBA in toluene were added to the mixture, and the solution was cooled to 50° C. The mixture was kept at this temperature for 3 hours, and then at 23° C. for a further 10 hours.

Provenance & Evidence