5-Bromoindole → HCID 4408258, compound

Participants

Reaction Steps

The title compound was prepared from 4-fluorobenzyl bromide and 5-bromoindole in substantially the same manner, as described in Step 1 of Example 25. The product was obtained as a white solid; mp: 57-58° C. Mass spectrum (APCI, [M+H]+) m/z 304. 1HNMR (400 MHz, DMSO-d6): δ 7.73 (d, 1H J=1.8 Hz), 7.55 (d, 1H, J=3.2 Hz), 7.43 (d, 1H, J=8.9 Hz), 7.24-7.19 (m, 3H), 7.12 (t, 2H, J=8.9 Hz), 6.47 (d, 1H, J=3.6 Hz), 5.40 (s, 2H), and 2.22 ppm (s, 3H). Elemental Analysis for C15H11BrFN: Calculated: C, 59.23; H, 3.65; N, 4.61. Found: C, 59.00; H, 3.55; N, 4.58.

Provenance & Evidence