(3-Methoxyphenyl)boronic acid → HCID 22032965, compound

Participants

Reaction Steps

The title compound was prepared from 5-bromo-1-[4-(tert-butyl)benzyl]-1H-indole (Step 1 of Example 34) and 3-methoxyphenylboronic acid in substantially the same manner, as described in Step 2 of Example 25. The product was obtained as an oil. Mass spectrum (ESI, [M+H]+) m/z 370. 1HNMR (400 MHz, DMSO-d6): δ 7.81 (s, 1H), 7.53 (s, 1H), 7.51 (d, 1H, J=8.55 Hz), 7.39 (d, 1H, J=8.55 Hz), 7.34-7.30 (m, 3H), 7.20 (d, 1H, J=7.64 Hz), 7.15-7.13 (m, 3H), 6.85 (d, 1H, J=8.25 Hz), 6.52 (d, 1H, J=3.05 Hz), 5.39 (s, 2H), 5.81 (s, 3H), and 1.21 ppm (s, 9H). Elemental Analysis for C26H27NO: Calculated: C, 84.51; H, 7.37; N, 3.79. Found: C, 83.30; H, 7.42; N, 3.74.

Provenance & Evidence