HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 5-Cyano-naphthalene-2-carboxylic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 69216040 | HCID 69216040 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 5-Cyano-naphthalene-2-carboxylic acid chloride | HCID 87737095 | — |
Reaction Steps
To a suspension of 5-cyano-naphthalene-2-carboxylic acid, 2, (0.084 g, 0.426 mmol) in CH2Cl2 (2 mL) at room temperature containing 1 drop of DMF is added oxalyl chloride (0.074 mL). Once the solution is homogeneous, the solution is concentrated in vacuo and the crude product is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07368462B1 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-abfba1fb62524b74bfcd758604b4e35b |
| Source note | uspto-grants-2008_05 |