HCID 68532101, compound → HCID 11544256, compound

HRID 2221311Notes

Reaction equation

HRID 2221311 reaction equation
Cl.[C:2]1([S:8]([C:11]2[CH:23]=[CH:22][C:14]3[O:15][C@@H:16]([CH2:19][NH:20][CH3:21])[CH2:17][O:18][C:13]=3[CH:12]=2)(=[O:10])=[O:9])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>CO>[C:2]1([S:8]([C:11]2[CH:23]=[CH:22][C:14]3[O:15][C@H:16]([CH2:19][NH:20][CH3:21])[CH2:17][O:18][C:13]=3[CH:12]=2)(=[O:10])=[O:9])[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 68532101HCID 68532101, compound

Product 1

HCID 11544256HCID 11544256, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Following the same procedure, (6-benzenesulfonyl-2,3-dihydro-benzo[1,4]dioxin-2-(S)-yl-methyl)-methyl amine hydrochloride salt was also prepared: MS; (M+H)+ 320, m. p. 209.0-212.0° C., [α]=−44° (methanol; c=0.5).

Workup

  1. customwas also prepared

Sources & evidence

ORD record
ord-e57b931e67e34887b8182aa2d5f94468
Source dataset
uspto-grants-2008_05
Patent number
US07368567B2

Reaction notes

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