Dimethylamine → HCID 58592600, compound

HRID 2222099Notes

Reaction equation

HRID 2222099 reaction equation
Cl.[CH3:2][O:3][C:4]([C:6]1[N:7]([CH3:13])[C:8]([CH2:11]Cl)=[N:9][CH:10]=1)=[O:5].[CH3:14][NH:15][CH3:16]>>[CH3:2][O:3][C:4]([C:6]1[N:7]([CH3:13])[C:8]([CH2:11][N:15]([CH3:16])[CH3:14])=[N:9][CH:10]=1)=[O:5]

Participants

3

Reactant 2

HCID 674DimethylamineHCID 67549831HCID 67549831, compound

Product 1

HCID 58592600HCID 58592600, compound

Procedure

Using 2-chloromethyl-3-methyl-3H-imidazole-4-carboxylic acid methyl ester hydrochloride and dimethylamine (33% solution in ethanol), the title compound was obtained as brown viscous oil (85% yield). MS: m/e=198(M+H+).

Sources & evidence

ORD record
ord-541ada1265ec4e03a849cd05e376b26c
Source dataset
uspto-grants-2008_05
Patent number
US07371749B2

Reaction notes

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