HCID 58592602, compound → HCID 43565333, compound

HRID 2222101Notes

Reaction equation

HRID 2222101 reaction equation
C([O:3][C:4]([C:6]1[CH:7]=[N:8][N:9]([CH2:11][CH2:12][N:13]([CH3:15])[CH3:14])[CH:10]=1)=[O:5])C.COCCN(CC1N(C)C(C(O)=O)=CN=1)C>>[CH3:14][N:13]([CH3:15])[CH2:12][CH2:11][N:9]1[CH:10]=[C:6]([C:4]([OH:5])=[O:3])[CH:7]=[N:8]1

Participants

3

Reactant 2

HCID 58592602HCID 58592602, compoundHCID 58592605HCID 58592605, compound

Product 1

HCID 43565333HCID 43565333, compoundYield 98%

Procedure

Using 1-(2-dimethylamino-ethyl)-1H-pyrazole-4-carboxylic acid ethyl ester, the title compound was prepared in the same manner as described for 2-{[(2-methoxy-ethyl)-methyl-amino]-methyl}-3-methyl-3H-imidazole-4-carboxylic acid. White solid (>98% yield by 1H-NMR). MS: m/e=184(M+H+).

Sources & evidence

ORD record
ord-862e16249e5b47aaae17e9522596b508
Source dataset
uspto-grants-2008_05
Patent number
US07371749B2

Reaction notes

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