HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 57457787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Diethyl phosphonomethanol | HCID 76513 | — |
| Reactant | 2-Methoxybenzoyl chloride | HCID 88969 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57457787 | HCID 57457787 | — |
Reaction Steps
A mixture of diethyl (hydroxymethyl)phosphonate (1.2 mmol), 2-anisoyl chloride (1 mmol) and pyridine (2 mmol) in 5 mL CH2Cl2 were stirred at rt for 4 h. Extraction and chromatography provided diethylphosphonomethyl 2-methoxybenzoate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371739B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-13cb4615d2794bff909c64b4b090bd95 |
| Source note | uspto-grants-2008_05 |