HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl chloroformate → 1,4-Dioxa-8-aza-spiro[4.5]decane-8-carboxylic acid (7-[1,4]dioxepan-6-yl-4-methoxy-benzothiazol-2-yl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | 1,4-Dioxa-8-azaspiro(4.5)decane | HCID 67435 | — |
| Reactant | 7-[1,4]Dioxepan-6-yl-4-methoxy-benzothiazol-2-ylamine | HCID 59711805 | — |
| Product | 1,4-Dioxa-8-aza-spiro[4.5]decane-8-carboxylic acid (7-[1,4]dioxepan-6-yl-4-methoxy-benzothiazol-2-yl)-amide | HCID 11351394 | — |
Reaction Steps
Using 7-[1,4]dioxepan-6-yl-4-methoxy-benzothiazol-2-ylamine, phenyl chloroformate and 1,4-dioxa-8-aza-spiro[4,5]decane, the title compound was prepared as off-white powder. MS: m/e=450(M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371748B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-55b01725f3a948d4be958c2e59fbeb81 |
| Source note | uspto-grants-2008_05 |