4-Methoxybenzoic Acid → N-(7-[1,4]Dioxepan-6-yl-4-methoxy-benzothiazol-2-yl)-4-methoxy-benzamide

HRID 2222144Notes

Reaction equation

HRID 2222144 reaction equation
[O:1]1[CH2:7][CH:6]([C:8]2[C:16]3[S:15][C:14]([NH2:17])=[N:13][C:12]=3[C:11]([O:18][CH3:19])=[CH:10][CH:9]=2)[CH2:5][O:4][CH2:3][CH2:2]1.[CH3:20][O:21][C:22]1[CH:30]=[CH:29][C:25]([C:26](O)=[O:27])=[CH:24][CH:23]=1>>[O:4]1[CH2:5][CH:6]([C:8]2[C:16]3[S:15][C:14]([NH:17][C:26](=[O:27])[C:25]4[CH:29]=[CH:30][C:22]([O:21][CH3:20])=[CH:23][CH:24]=4)=[N:13][C:12]=3[C:11]([O:18][CH3:19])=[CH:10][CH:9]=2)[CH2:7][O:1][CH2:2][CH2:3]1

Participants

3

Reactant 2

HCID 74784-Methoxybenzoic AcidHCID 597118057-[1,4]Dioxepan-6-yl-4-methoxy-benzothiazol-2-ylamine

Product 1

HCID 11429903N-(7-[1,4]Dioxepan-6-yl-4-methoxy-benzothiazol-2-yl)-4-methoxy-benzamide

Procedure

Using 7-[1,4]dioxepan-6-yl-4-methoxy-benzothiazol-2-ylamine and 4-methoxy-benzoic acid, the title compound was prepared as white powder. MS: m/e=415(M+H+).

Sources & evidence

ORD record
ord-564ae2da6e1a49799f28dc9a25e421ff
Source dataset
uspto-grants-2008_05
Patent number
US07371748B2

Reaction notes

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