Phenyl chloroformate → HCID 86595143, compound

HRID 2222162Notes

Reaction equation

HRID 2222162 reaction equation
[O:1]1[CH2:7][CH:6]([C:8]2[C:16]3[S:15][C:14]([NH2:17])=[N:13][C:12]=3[C:11]([O:18][CH3:19])=[CH:10][CH:9]=2)[CH2:5][O:4][CH2:3][CH2:2]1.Cl[C:21](OC1C=CC=CC=1)=[O:22].[OH:30][CH2:31][C:32]1([CH3:38])[CH2:37][CH2:36][NH:35][CH2:34][CH2:33]1>>[O:4]1[CH2:5][CH:6]([C:8]2[C:16]3[S:15][C:14]([NH:17][C:21]([N:35]4[CH2:36][CH2:37][C:32]([CH2:31][OH:30])([CH3:38])[CH2:33][CH2:34]4)=[O:22])=[N:13][C:12]=3[C:11]([O:18][CH3:19])=[CH:10][CH:9]=2)[CH2:7][O:1][CH2:2][CH2:3]1

Participants

4

Reactant 3

HCID 15891Phenyl chloroformateHCID 22507737(4-Methylpiperidin-4-yl)methanolHCID 597118057-[1,4]Dioxepan-6-yl-4-methoxy-benzothiazol-2-ylamine

Product 1

HCID 86595143HCID 86595143, compound

Procedure

Using 7-[1,4]dioxepan-6-yl-4-methoxy-benzothiazol-2-ylamine, phenyl chloroformate and 4-hydroxymethyl-4-methyl-piperidine, the title compound was prepared as light brown powder. MS: m/e=436(M+H+).

Sources & evidence

ORD record
ord-ebfe4cfd27fc47dba348e7848f68614b
Source dataset
uspto-grants-2008_05
Patent number
US07371748B2

Reaction notes

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