3,4-Dimethoxybenzeneacetonitrile → HCID 23089843, compound

HRID 2222336Notes

Reaction equation

HRID 2222336 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH:5]=O.[CH3:10][O:11][C:12]1[CH:13]=[C:14]([CH:18]=[CH:19][C:20]=1[O:21][CH3:22])[CH2:15][C:16]#[N:17]>>[CH3:10][O:11][C:12]1[CH:13]=[C:14](/[C:15](=[CH:5]/[C:4]2[CH:7]=[CH:8][CH:9]=[C:2]([F:1])[CH:3]=2)/[C:16]#[N:17])[CH:18]=[CH:19][C:20]=1[O:21][CH3:22]

Participants

3

Reactant 2

HCID 667273,4-DimethoxybenzeneacetonitrileHCID 680093-Fluorobenzaldehyde

Product 1

HCID 23089843HCID 23089843, compoundYield 15.3%

Procedure

3-Fluorobenzaldehyde (2.0 g) and 3,4-dimethoxybenzyl cyanide (2.9 g) were subjected to condensation in accordance with process A of (production process 2), to thereby produce the target product (0.7 g, yield: 15%).

Sources & evidence

ORD record
ord-8af7434cc51f409697ba4ec27aac48e9
Source dataset
uspto-grants-2008_05
Patent number
US07371773B2

Reaction notes

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