2-Nitrobenzaldehyde → HCID 10041035, compound

HRID 2222358Notes

Reaction equation

HRID 2222358 reaction equation
[N+:1]([C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=O)([O-:3])=[O:2].[CH3:12][O:13][C:14]1[CH:15]=[C:16]([CH:20]=[CH:21][C:22]=1[O:23][CH3:24])[CH2:17][C:18]#[N:19]>>[CH3:12][O:13][C:14]1[CH:15]=[C:16](/[C:17](=[CH:6]/[C:5]2[CH:8]=[CH:9][CH:10]=[CH:11][C:4]=2[N+:1]([O-:3])=[O:2])/[C:18]#[N:19])[CH:20]=[CH:21][C:22]=1[O:23][CH3:24]

Participants

3

Reactant 2

HCID 111012-NitrobenzaldehydeHCID 667273,4-Dimethoxybenzeneacetonitrile

Product 1

HCID 10041035HCID 10041035, compoundYield 84%

Procedure

2-Nitrobenzaldehyde (1.51 g) and 3,4-dimethoxybenzyl cyanide (1.77 g) were subjected to condensation in accordance with process A of (production process 2), to thereby produce the target product (2.59 g, yield: 84%).

Sources & evidence

ORD record
ord-dfc0e914ff7946b7a87f3add92fe777b
Source dataset
uspto-grants-2008_05
Patent number
US07371773B2

Reaction notes

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