HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2222573Generated: October 30, 2026
2-Methoxyethylamine → HCID 54013946, compound
https://huagongshe.com/reaction/2222573
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 6-Chloropurine riboside | HCID 93003 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54013946 | HCID 54013946 | 98% |
Reaction Steps
547 mg 6-chloropurine riboside, 0.882 mL 2-methoxyethylamine, and 5.0 mL ethyl alcohol are combined and heated to 90° C. in a sealed reaction vessel for about 22 hours. The ligand is then purified by silica gel chromatography using 8:1 methylene chloride:methanol to yield N6-(2-methoxyethyl)-adenosine (0.61 g, 98% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07371852B2 |
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| Source dataset | uspto-grants-2008_05 |
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| ORD ID | ord-f7f7bca8282e4f5e9ba1eaa046a68e78 |
|---|
| Source note | uspto-grants-2008_05 |
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