7-Amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one → HCID 69284257, compound

HRID 2223276Notes

Reaction equation

HRID 2223276 reaction equation
[NH2:1][CH:2]1[C:8](=[O:9])[N:7]([CH3:10])[C:6]2[CH:11]=[CH:12][CH:13]=[CH:14][C:5]=2[C:4]2[CH:15]=[CH:16][CH:17]=[CH:18][C:3]1=2.[CH3:19][O:20][C:21]1[CH:35]=[CH:34][C:24]([CH2:25][NH:26][C:27](=[O:33])[CH:28]([CH3:32])[C:29](O)=[O:30])=[CH:23][CH:22]=1>>[CH3:19][O:20][C:21]1[CH:22]=[CH:23][C:24]([CH2:25][NH:26][C:27](=[O:33])[CH:28]([CH3:32])[C:29]([NH:1][CH:2]2[C:8](=[O:9])[N:7]([CH3:10])[C:6]3[CH:11]=[CH:12][CH:13]=[CH:14][C:5]=3[C:4]3[CH:15]=[CH:16][CH:17]=[CH:18][C:3]2=3)=[O:30])=[CH:34][CH:35]=1

Participants

3

Reactant 2

HCID 101986267-Amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-oneHCID 69280637HCID 69280637, compound

Product 1

HCID 69284257HCID 69284257, compound

Procedure

The title compound, MS: m/e=458.3 (M+H+), was prepared in analogy to example 16 from 7-amino-5-methyl-5H,7H-dibenzo[b,d]azepin-6-one and N-(4-methoxy-benzyl)-2-methyl-malonamic acid.

Sources & evidence

ORD record
ord-1b00f3ac05e3413185aa9325cca5ff78
Source dataset
uspto-grants-2008_05
Patent number
US07375099B2

Reaction notes

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