7-Amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one → HCID 69282780, compound

HRID 2223278Notes

Reaction equation

HRID 2223278 reaction equation
[NH2:1][CH:2]1[C:8](=[O:9])[N:7]([CH3:10])[C:6]2[CH:11]=[CH:12][CH:13]=[CH:14][C:5]=2[C:4]2[CH:15]=[CH:16][CH:17]=[CH:18][C:3]1=2.[CH3:19][O:20][C:21]1[CH:22]=[C:23]([CH:33]=[CH:34][C:35]=1[O:36][CH3:37])[CH2:24][NH:25][C:26](=[O:32])[CH:27]([CH3:31])[C:28](O)=[O:29]>>[CH3:19][O:20][C:21]1[CH:22]=[C:23]([CH:33]=[CH:34][C:35]=1[O:36][CH3:37])[CH2:24][NH:25][C:26](=[O:32])[CH:27]([CH3:31])[C:28]([NH:1][CH:2]1[C:8](=[O:9])[N:7]([CH3:10])[C:6]2[CH:11]=[CH:12][CH:13]=[CH:14][C:5]=2[C:4]2[CH:15]=[CH:16][CH:17]=[CH:18][C:3]1=2)=[O:29]

Participants

3

Reactant 2

HCID 101986267-Amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-oneHCID 69280721HCID 69280721, compound

Product 1

HCID 69282780HCID 69282780, compound

Procedure

The title compound, MS: m/e=488.3 (M+H+), was prepared in analogy to example 16 from 7-amino-5-methyl-5H,7H-dibenzo[b,d]azepin-6-one and N-(3,4-dimethoxy-benzyl)-2-methyl-malonamic acid.

Sources & evidence

ORD record
ord-c0a47d64b7d24efc94726f8b7d0d70f1
Source dataset
uspto-grants-2008_05
Patent number
US07375099B2

Reaction notes

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