7-Amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one → HCID 69283583, compound

HRID 2223285Notes

Reaction equation

HRID 2223285 reaction equation
[NH2:1][CH:2]1[C:8](=[O:9])[N:7]([CH3:10])[C:6]2[CH:11]=[CH:12][CH:13]=[CH:14][C:5]=2[C:4]2[CH:15]=[CH:16][CH:17]=[CH:18][C:3]1=2.[CH3:19][CH:20]([C:24]([NH:26][CH2:27][C:28]1[CH:33]=[C:32]([O:34][CH3:35])[CH:31]=[C:30]([O:36][CH3:37])[CH:29]=1)=[O:25])[C:21](O)=[O:22]>>[CH3:37][O:36][C:30]1[CH:29]=[C:28]([CH:33]=[C:32]([O:34][CH3:35])[CH:31]=1)[CH2:27][NH:26][C:24](=[O:25])[CH:20]([CH3:19])[C:21]([NH:1][CH:2]1[C:8](=[O:9])[N:7]([CH3:10])[C:6]2[CH:11]=[CH:12][CH:13]=[CH:14][C:5]=2[C:4]2[CH:15]=[CH:16][CH:17]=[CH:18][C:3]1=2)=[O:22]

Participants

3

Reactant 2

HCID 101986267-Amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-oneHCID 69282720HCID 69282720, compound

Product 1

HCID 69283583HCID 69283583, compound

Procedure

The title compound, MS: m/e=488.3 (M+H+), was prepared in analogy to example 16 from 7-amino-5-methyl-5H,7H-dibenzo[b,d]azepin-6-one and 2-methyl-N-(3,5-dimethoxy-benzyl)-malonamic acid.

Sources & evidence

ORD record
ord-e25d18547356465696b39496712338ba
Source dataset
uspto-grants-2008_05
Patent number
US07375099B2

Reaction notes

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