HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 59715317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 59715291 | HCID 59715291 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 59715317 | HCID 59715317 | 60% |
Reaction Steps
The biphenyl (0.235 mg, 1.0 equiv) was dissolved in CCl4 (5 mL), NBS added, and the solution was irradiated until starting material was consumed. The mixture was allowed to cool to room temperature and then filtered through celite. The filtrate was concentrated and the residue purified by column chromatography (SiO2, hexane) to give the desired product (0.258 g, 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07375125B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-5cbdacb2eaea4c8f971d80b25f649534 |
| Source note | uspto-grants-2008_05 |