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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2223323Generated: October 30, 2026

N-bromobutanimide → HCID 59715317, compound

https://huagongshe.com/reaction/2223323

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-bromobutanimideHCID 67184—
ReactantHCID 59715291HCID 59715291—
SolventCarbon TetrachlorideHCID 5943—
ProductHCID 59715317HCID 5971531760%

Reaction Steps

The biphenyl (0.235 mg, 1.0 equiv) was dissolved in CCl4 (5 mL), NBS added, and the solution was irradiated until starting material was consumed. The mixture was allowed to cool to room temperature and then filtered through celite. The filtrate was concentrated and the residue purified by column chromatography (SiO2, hexane) to give the desired product (0.258 g, 60%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07375125B2
Source datasetuspto-grants-2008_05
ORD IDord-5cbdacb2eaea4c8f971d80b25f649534
Source noteuspto-grants-2008_05