HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Trifluoromethyl)trimethylsilane → HCID 131726884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Trifluoromethyl)trimethylsilane | HCID 552549 | — |
| Reactant | HCID 69105192 | HCID 69105192 | — |
| Product | HCID 131726884 | HCID 131726884 | — |
Reaction Steps
In the reaction with (trifluoromethyl)-trimethylsilane analogously to instructions 1.1, 135 mg of alcohol 16c yields 159 mg of trimethylsilyl ether 17c as a yellow, viscous mass (GC-MS: m/z theor.: 748, pract.: 748). The latter is, without the reaction being performed with tetrabutylammonium fluoride-trihydrate, used in the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07375098B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-8fd43f6e68dc4c38abf5cd9781a13fdc |
| Source note | uspto-grants-2008_05 |