HuagongsheHuagongshe Chemistry Print Report · For research reference only
11beta-[5-(Methylamino)pentyl]-8-vinylestra-1,3,5(10)-triene-3,17beta-diol → 11beta-{5-[Methyl(8,8,9,9,9-pentafluorononyl)amino]pentyl}-8-vinylestra-1,3,5(10)-triene-3,17beta-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11beta-[5-(Methylamino)pentyl]-8-vinylestra-1,3,5(10)-triene-3,17beta-diol | HCID 12136542 | — |
| Reactant | HCID 15858643 | HCID 15858643 | — |
| Product | 11beta-{5-[Methyl(8,8,9,9,9-pentafluorononyl)amino]pentyl}-8-vinylestra-1,3,5(10)-triene-3,17beta-diol | HCID 12136547 | — |
Reaction Steps
In the reaction with 8,8,9,9,9-pentafluorononyltosylate analogously to instructions 22.1, 32 mg of amine 31a yields 16 mg of amine 36a as colorless crystals (GC-MS: m/z theor.: 613, pract.: 613).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07375098B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-074ee115e7384dfe8c52ead0cedefa7c |
| Source note | uspto-grants-2008_05 |