6-Chloro-1,2,3,4-tetrahydro(1)benzothieno(2,3-c)pyridine → HCID 58659042, compound

HRID 2223498Notes

Reaction equation

HRID 2223498 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[S:14][C:9]3[CH2:10][NH:11][CH2:12][CH2:13][C:8]=3[C:6]=2[CH:7]=1.[CH2:15]([N:17]([CH2:30][CH3:31])[C:18]1[CH:26]=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][C:19]=1[C:20](O)=[O:21])[CH3:16]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[S:14][C:9]3[CH2:10][N:11]([C:20]([C:19]4[CH:23]=[C:24]([N+:27]([O-:29])=[O:28])[CH:25]=[CH:26][C:18]=4[N:17]([CH2:30][CH3:31])[CH2:15][CH3:16])=[O:21])[CH2:12][CH2:13][C:8]=3[C:6]=2[CH:7]=1

Participants

3

Procedure

The title compound was prepared in analogy to Example 1 using 6-chloro-1,2,3,4-tetrahydro-[1]benzothieno[2,3-c]pyridine [29078-50-0] and 2-(diethylamino)-5-nitro-benzoic acid [727718-14-1]. MS (m/e): 444.1 (M+H+).

Sources & evidence

ORD record
ord-ed84c8a4a57f4943af5fd602d1eef6f4
Source dataset
uspto-grants-2008_05
Patent number
US07375226B2

Reaction notes

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