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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2223601Generated: October 30, 2026

HCID 68537658, compound → HCID 68540296, compound

https://huagongshe.com/reaction/2223601

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68537658HCID 68537658—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 68540296HCID 68540296101.4%

Reaction Steps

3-(2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyloxy)-4-{[4-(2-benzyloxycarbonyl-2-methylpropoxy)phenyl]methyl}-5-isopropy-1H-pyrazole (0.28 g) was dissolved in methanol (6 mL). To the solution was added 10% palladium-carbon powder (54 mg), and the mixture was stirred at room temperature under a hydrogen atmosphere overnight. The insoluble material was removed by filtration, and the solvent of the filtrate was removed under reduced pressure to give the title compound (0.25 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07375087B2
Source datasetuspto-grants-2008_05
ORD IDord-661c02d474244812ba91781a28a56674
Source noteuspto-grants-2008_05