HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 2-amino-2-methylpropanoate hydrochloride → Benzyl 2-amino-2-methylpropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 2-amino-2-methylpropanoate hydrochloride | HCID 21415531 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Benzyl 2-amino-2-methylpropanoate | HCID 11116894 | 96.4% |
Reaction Steps
Benzyl 2-amino-2-methylpropionate hydrochloride (1.48 g) was dissolved in ethyl acetate (60 mL) and a saturated aqueous sodium hydrogen carbonate solution (20 mL), and the organic layer was separated. The organic layer was washed with brine, and dried over anhydrous magnesium sulfate. The solvent was removed under reduced pressure to give the title compound (1.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07375087B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-c2d94bb84f8d4e2e9fb78401bd10114c |
| Source note | uspto-grants-2008_05 |