L-Aspartic Acid → 21059-46-1
Reaction equation
[Ca:1].[NH2:2][C@H:3]([C:8]([OH:10])=[O:9])[CH2:4][C:5]([OH:7])=[O:6]>O>[Ca:1].[NH2:2][C@H:3]([C:8]([OH:10])=[O:9])[CH2:4][C:5]([OH:7])=[O:6]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
20 g of seaweed calcium (calcium content: 32%) was dispersed in 500 ml of water and dissolved therein by stirring, and 60 g of aspartic acid was added thereto to perform a reaction, then the solution was continually stirred until the seaweed calcium and aspartic acid were entirely dissolved. Bubbles were generated in the initial stage of the reaction but they disappeared after a certain time. The resulting reaction solution was centrifuged to remove insoluble materials, and the clear supernatant was separated. The supernatant was freeze-dried to obtain about 72 g of seaweed calcium-aspartic acid chelate.
Workup
- dissolutiondissolved
- customa reaction
- dissolutionwere entirely dissolved
- customstage of the reaction but they
- customThe resulting reaction solution
- customto remove insoluble materials
- customthe clear supernatant was separated
- customThe supernatant was freeze-dried
Sources & evidence
- ORD record
- ord-58fb21afa0f249e194f862dcee19138e
- Source dataset
- uspto-grants-2008_05
- Patent number
- US07375243B2
Reaction notes
Loading…