Carbazole → 4-(9H-Carbazol-9-yl)butanenitrile

HRID 222393Notes

Reaction equation

[CH:1]1[C:13]2[NH:12][C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5]=2[CH:4]=[CH:3][CH:2]=1.Br[CH2:15][CH2:16][CH2:17][C:18]#[N:19]>>[CH:10]1[C:11]2[N:12]([CH2:15][CH2:16][CH2:17][C:18]#[N:19])[C:13]3[C:5](=[CH:4][CH:3]=[CH:2][CH:1]=3)[C:6]=2[CH:7]=[CH:8][CH:9]=1

Participants

Reactant 2

HCID 6854Carbazole

HCID 214124-Bromobutyronitrile

Product 1

HCID 283681154-(9H-Carbazol-9-yl)butanenitrile

Procedure

Carbazole (10 g, 0.060 mol) was reacted with 4-bromobutyronitrile (11.9 ml, 0.12 mol) by working in a similar manner to Example 1a).

Sources & evidence

ORD record: ord-e56a4e6027834f258ccf92ddca195c8d
Source dataset: uspto-grants-2012_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08207214B2

Reaction notes

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