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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2224032Generated: October 30, 2026

[(3S,6R)-6-(6-azido-hexyloxy)-1-methyl-2-oxo-azepan-3-yl]-carbamic acid tert-butyl ester → (3S,6S)-3-amino-6-azido-azepan-2-one

https://huagongshe.com/reaction/2224032

Reaction equation

Participants

RoleNameHCIDCharge
Reactant[(3S,6R)-6-(6-azido-hexyloxy)-1-methyl-2-oxo-azepan-3-yl]-carbamic acid tert-butyl esterHCID 86609579—
Reactant((3S,6S)-6-azido-2-oxo-azepan-3-yl)-carbamic acid tert-butyl esterHCID 86609581—
Product(3S,6S)-3-amino-6-azido-azepan-2-oneHCID 86609582—

Reaction Steps

Following the procedure of example 2d) ((3S,6S)-6-azido-2-oxo-azepan-3-yl)-carbamic acid tert-butyl ester is substituted for [(3S,6R)-6-(6-azido-hexyloxy)-1-methyl-2-oxo-azepan-3-yl]-carbamic acid tert-butyl ester to give (3S,6S)-3-amino-6-azido-azepan-2-one. MS (ESI) 170 (M+H)+

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07378410B2
Source datasetuspto-grants-2008_05
ORD IDord-104510962f5d4b629f12561a374cd650
Source noteuspto-grants-2008_05