HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(5-chloro-2-vinyl-phenyl)-acetamide → 6-Acetyl-2,8-dichloro-3-fluoro-5,6-dihydropyrido[3,2-c][1]benzazocine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(5-chloro-2-vinyl-phenyl)-acetamide | HCID 21767401 | — |
| Reactant | 3-(Bromomethyl)-2,6-dichloro-5-fluoropyridine | HCID 59717573 | — |
| Reactant | 6-Acetyl-2-chloro-3-fluoro-5,6-dihydro-pyrido[3,2-c][1]benzazocine | HCID 74393412 | — |
| Product | 6-Acetyl-2,8-dichloro-3-fluoro-5,6-dihydropyrido[3,2-c][1]benzazocine | HCID 85424790 | — |
Reaction Steps
Compound 6D was prepared from 6C and 1B in two steps by a route analogous to that used for the preparation of 1D. HPLC Rt=3.032 min; LCMS Found: (M+H)+=337.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-33c5f1fa66a243acb23b9629c65e8255 |
| Source note | uspto-grants-2008_05 |