HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Bromomethyl)-2,6-dichloro-5-fluoropyridine → 6-Acetyl-2,9-dichloro-3-fluoro-5,6-dihydropyrido[3,2-c][1]benzazocine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Bromomethyl)-2,6-dichloro-5-fluoropyridine | HCID 59717573 | — |
| Reactant | N-(4-chloro-2-vinyl-phenyl)-acetamide | HCID 59717611 | — |
| Reactant | 6-Acetyl-2-chloro-3-fluoro-5,6-dihydro-pyrido[3,2-c][1]benzazocine | HCID 74393412 | — |
| Product | 6-Acetyl-2,9-dichloro-3-fluoro-5,6-dihydropyrido[3,2-c][1]benzazocine | HCID 72366778 | — |
Reaction Steps
Compound 9C was prepared from 9B and 1B by a route analogous to that used for the preparation of 1D. HPLC Rt=3.146 min; LCMS Found: (M+H)+=337.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-e89944e73a564de2a45d6921b4e25929 |
| Source note | uspto-grants-2008_05 |