3-(Bromomethyl)-2-chloropyridine → HCID 69292975, compound

HRID 2224316Notes

Reaction equation

HRID 2224316 reaction equation
BrCC1C(Cl)=NC=CC=1.[C:10]([N:13]1[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[CH:18]=[CH:17][C:16]2[N:25]=[C:26](Cl)[C:27](F)=[CH:28][C:15]=2[CH2:14]1)(=[O:12])[CH3:11]>>[C:10]([N:13]1[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[CH:18]=[CH:17][C:16]2[N:25]=[CH:26][CH:27]=[CH:28][C:15]=2[CH2:14]1)(=[O:12])[CH3:11]

Participants

3

Reactant 2

HCID 189310283-(Bromomethyl)-2-chloropyridineHCID 743934126-Acetyl-2-chloro-3-fluoro-5,6-dihydro-pyrido[3,2-c][1]benzazocine

Product 1

HCID 69292975HCID 69292975, compound

Procedure

Compound 12C was prepared from bb and 12B by a route analogous to that used for the preparation of 1D. HPLC Rt=1.326 min; LCMS Found: (M+H)+=251.

Sources & evidence

ORD record
ord-0e260d0d096f417daa13580c667e28ae
Source dataset
uspto-grants-2008_05
Patent number
US07378426B2

Reaction notes

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