HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2,6-Dichloropyridin-3-yl)methanol → 3-(Bromomethyl)-2,6-dichloropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2,6-Dichloropyridin-3-yl)methanol | HCID 12259932 | — |
| Reactant | 3-(Bromomethyl)-2,6-dichloro-5-fluoropyridine | HCID 59717573 | — |
| Product | 3-(Bromomethyl)-2,6-dichloropyridine | HCID 12265394 | 80% |
Reaction Steps
Compound 13B (0.88 g, 80%) was prepared from 13A (0.82 g, 4.6 mmol) using a procedure similar to the synthesis of 1B. HPLC Rt=2.44 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-1c1b1d9f2abd4e32abc23d47397accaf |
| Source note | uspto-grants-2008_05 |